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API TR 13M-5 Procedure for Testing and Evaluating the Performance of Friction (Drag) Reducers in Aqueous-based Fluid Flowing in Straight, Smooth Circular Conduits, First Edition

standard by American Petroleum Institute, 10/01/2018

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API TR 13M-5 provides a consistent methodology to test and evaluate the performance of friction (drag) reducers in straight, smooth circular conduits. This standard includes only smooth-walled tubing and excludes any rough-walled tubing.

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Procedure for Testing and Evaluating the Performance of Friction (Drag) Reducers in Aqueous-based Fluid Flowing in Straight, Smooth Circular Conduits


API TECHNICAL REPORT 13M-5 FIRST EDITION, OCTOBER 2018




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Copyright © 2018 American Petroleum Institute


Foreword


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This document was produced under API standardization procedures that ensure appropriate notification and participation in the developmental process and is designated as an API technical report. Questions concerning the interpretation of the content of this publication or comments and questions concerning the procedures under which this publication was developed should be directed in writing to the Director of Standards, American Petroleum Institute, 1220 L Street, NW, Washington, DC 20005. Requests for permission to reproduce or translate all or any part of the material published herein should also be addressed to the director.


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Suggested revisions are invited and should be submitted to the Standards Department, API, 1220 L Street, NW, Washington, DC 20005, standards@api.org.


iii


Contents


Page

  1. Scope 1

  2. Terms and Definitions 1

  3. Measurement and Precision 2

  4. Instrument Calibration 2

  5. Friction Loop Calibration 2

    1. Introduction 2

    2. Flow Loop Schematic 2

    3. Calibration Procedure 3

    4. Calibration Data Analysis 3

    5. Determination of the Internal Tubing or Pipe Diameter (di) 4

    6. Calibration Example—Determination of Internal Pipe Diameter 5

  6. Fluid Preparation, Testing, and Analysis 7

    1. Base Fluid 7

    2. Test Fluid 7

    3. Fluid Testing 8

    4. Data Analysis 8

    5. Example—Friction Reducer Fluid Analysis 8

Annex A (informative) List of Symbols and Conversion factors 12

Bibliography 13

Figures

  1. Typical Flow Loop System (Schematic) 2

  2. Plot of Wall Shear Stress vs Wall Shear Rate for Fresh Water Solvent 6

  3. Plot of Fanning Friction Factor vs Solvent Reynolds Number for Fresh Water 7

  4. Plot of Fanning Friction Factor vs Friction Reducer Fluid Reynolds Number 10

  5. Plot of Drag Reduction vs Friction Reducer Fluid Reynolds Number 10

  6. Plot of Drag Reduction vs Velocity for Friction Reducer Fluid 11

  7. Plot of Drag Reduction vs Wall Shear Rate for Friction Reducer Fluid 11

Tables

  1. Calibration Test Data 5

  2. Calibration Test Calculations 6

  3. Friction Reducer Test Fluid Data 9

  4. Friction Reducer Test Fluid Calculations 9

A.1 Symbols, Definitions, and Units 12


v


Introduction


The objective of this document is to provide a standard procedure for testing and evaluating the performance of friction (drag) reducers in straight, smooth circular conduits. This standard procedure was compiled on the basis of several years of comparative testing, debate, discussion, and continued research by the industry.


In this standard, where practical, US Customary units are included in brackets for information. The units do not necessarily represent a direct conversion of SI to US Customary units, or US Customary to SI. Consideration has been given to the precision of the instrument making the measurement. For example, thermometers are typically marked in one degree increments, thus temperature values have been rounded to the nearest degree.


This document uses a format for numbers which follows the examples given in API Document Format and Style Manual (Revision Date: November 2017). In this document, the decimal mark is a period and separates the whole part from the fractional part of a number. No spaces are used in the numbering format. The thousands separator is a comma and is only used for numbers greater than 10,000 (i.e. 5000 items, 12,500 bags).


vi


Procedure for Testing and Evaluating the Performance of Friction (Drag) Reducers in Aqueous-based Fluid Flowing in Straight, Smooth Circular Conduits


  1. Scope

    1. This document provides a consistent methodology to test and evaluate the performance of friction (drag) reducers in straight, smooth circular conduits. This standard includes only smooth-walled tubing and excludes any rough-walled tubing.


    2. The International System of Units (SI) is used in this Technical Report. However, testing data acquisition can be conducted using US customary units (USC).


    3. Factors included in Annex A Table A.1 permit conversions of USC units to SI units or SI units to USC units.


  2. Terms and Definitions

For the purposes of this document, the following terms and definitions apply.


2.1

base fluid

Aqueous liquid media (solvent with or without additives) used to prepare test fluid (see 2.8).


2.2

friction reducer

Agent that dissolves in base fluid, thereby reducing frictional resistance to flow.


2.3

straight, smooth circular conduits

Metallic-based smooth-walled straight tubing or pipe having a constant diameter.


2.4

drag reduction friction reduction

Relative reduction in the change in pressure due to frictional resistance by the addition of friction reducer to the base fluid.


2.5

Reynolds number (NRe)

The ratio of inertial forces to viscous forces within a fluid (a dimensionless number).


2.6

Fanning friction factor ( f )

For a fluid, the ratio of pipe wall shear stress to the flow kinetic energy (a dimensionless number).


2.7

solvent

Aqueous liquid used to prepare the test fluid (water, brine, etc.) and the fluid used to determine the internal diameter of the tubing or pipe (see 5.3).


NOTE For the purpose of the document, for determination of internal diameter of the tubing or pipe, the solvent is fresh water.


2.8

test fluid

Fluid prepared with the base fluid and the friction reducer.


1